Real-time analysis of Pd2(dba)3 activation by phosphine ligands

Date

2017-01

Authors

Janusson, Eric
Zijlstra, Harmen S.
Nguyen, Peter P.T.
MacGillivray, Landon
Martelino, Julio
McIndoe, J. Scott

Journal Title

Journal ISSN

Volume Title

Publisher

Chemical Communications

Abstract

A combination of UV-Vis spectroscopy and electrospray ionization mass spectrometry is used for real-time monitoring of Pd2(dba)3 activation with sulfonated versions of PPh3 and Buchwald-type ligands. This provides insight into the effect of ligand and preparation conditions on activation and allows for establishment of rational activation protocols.

Description

Keywords

Citation

Janusson, E., Zijlstra, H.S., Nguyen, P.P.T., MacGillivray, L. Martelino, J. & McIndoe, J.S. (2017). Real-time analysis of Pd2(dba)3 activation by phosphine ligands. Chemical Communications, 53(5), 854-856. https://doi.org/10.1039/C6CC08824D