Pressurized Sample Infusion

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dc.contributor.authorThomas, Gilian T.
dc.contributor.authorDonnecke, Sofia
dc.contributor.authorChagunda, Ian C.
dc.contributor.authorMcIndoe, J. Scott
dc.date.accessioned2022-02-23T23:52:31Z
dc.date.available2022-02-23T23:52:31Z
dc.date.copyright2022en_US
dc.date.issued2021-12-15
dc.descriptionThanks to all of the students who developed and refined the PSI technique over the years, especially Krista Kobylianskii, Zohrab Ahmadi, Jingwei Luo, Rhonda Stoddard, Lars Yunker, Eric Janusson, Robin Theron, Anuj Joshi, and Isaac Omari.en_US
dc.description.abstractPressurized sample infusion (PSI) is a simple and effective means of continuously introducing a solution to an electrospray ionization mass spectrometry (ESI-MS) source. It allows for acquisition of real-time data in an air- and moisture-free environment and requires minimal additional infrastructure. It is applicable for use for any reaction in which one or more components are detectable by ESI-MS and for which time-course information is desired over a time scale of seconds to minutes. The strengths and weaknesses of the method are critically examined, and technique tips and tricks are provided to enable maximal effectiveness when employing this approach to continuous monitoring of complex reaction mixtures.en_US
dc.description.reviewstatusRevieweden_US
dc.description.scholarlevelFacultyen_US
dc.description.sponsorshipJ. S. M. thanks the NSERC Discovery program for operational funding and CFI, BCKDF and the University of Victoria for infrastructural supporten_US
dc.identifier.citationThomas, G.T., Donnecke, S., Chagunda, I.C., & McIndoe, J. S. (2021). Chemistry Methods, 2(1), https://doi.org/10.1002/cmtd.202100068en_US
dc.identifier.urihttps://doi.org/10.1002/cmtd.202100068
dc.identifier.urihttp://hdl.handle.net/1828/13756
dc.language.isoenen_US
dc.publisherChemistry-Methodsen_US
dc.subjectmass spectrometry
dc.subjecton-line monitoring
dc.subjectpressurized sample infusion
dc.subjectreaction mechanisms
dc.subjectreal-time monitoring
dc.subject.departmentSchool of Environmental Studies
dc.subject.departmentDepartment of History
dc.subject.departmentDepartment of Biology
dc.titlePressurized Sample Infusionen_US
dc.typeArticleen_US

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